A novel route in the synthesis of magnetite nanoparticles

Mira Ristić; Tatsuo Fujii; Hideki Hashimoto; Ivana Opačak; Svetozar Musić

doi:10.1016/j.matlet.2013.03.013

A novel route in the synthesis of magnetite nanoparticles

Mira Ristić, Tatsuo Fujii, Hideki Hashimoto, Ivana Opačak, Svetozar Musić

Research output: Contribution to journal › Article › peer-review

16 Citations (Scopus)

Abstract

A novel route in the synthesis of magnetite nanoparticles is reported. This synthesis is based on autoclaving of iron choline citrate dissolved in mixed water/ethanol or water solution and neutralized with NH₄OH solution. The magnetite precipitates were characterized by XRD, Mössbauer, FT-IR, HRTEM and magnetometric measurements. All the precipitated magnetite particles were in the nanosize range as shown by HRTEM. They did not contain organic residues or any other iron (hydrous) oxide phase.

Original language	English
Pages (from-to)	93-97
Number of pages	5
Journal	Materials Letters
Volume	100
DOIs	https://doi.org/10.1016/j.matlet.2013.03.013
Publication status	Published - Apr 8 2013

Keywords

HRTEM
Magnetite
Magnetometry
Mössbauer
XRD

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/j.matlet.2013.03.013

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title = "A novel route in the synthesis of magnetite nanoparticles",

abstract = "A novel route in the synthesis of magnetite nanoparticles is reported. This synthesis is based on autoclaving of iron choline citrate dissolved in mixed water/ethanol or water solution and neutralized with NH4OH solution. The magnetite precipitates were characterized by XRD, M{\"o}ssbauer, FT-IR, HRTEM and magnetometric measurements. All the precipitated magnetite particles were in the nanosize range as shown by HRTEM. They did not contain organic residues or any other iron (hydrous) oxide phase.",

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T1 - A novel route in the synthesis of magnetite nanoparticles

AU - Ristić, Mira

AU - Fujii, Tatsuo

AU - Hashimoto, Hideki

AU - Opačak, Ivana

AU - Musić, Svetozar

PY - 2013/4/8

Y1 - 2013/4/8

N2 - A novel route in the synthesis of magnetite nanoparticles is reported. This synthesis is based on autoclaving of iron choline citrate dissolved in mixed water/ethanol or water solution and neutralized with NH4OH solution. The magnetite precipitates were characterized by XRD, Mössbauer, FT-IR, HRTEM and magnetometric measurements. All the precipitated magnetite particles were in the nanosize range as shown by HRTEM. They did not contain organic residues or any other iron (hydrous) oxide phase.

AB - A novel route in the synthesis of magnetite nanoparticles is reported. This synthesis is based on autoclaving of iron choline citrate dissolved in mixed water/ethanol or water solution and neutralized with NH4OH solution. The magnetite precipitates were characterized by XRD, Mössbauer, FT-IR, HRTEM and magnetometric measurements. All the precipitated magnetite particles were in the nanosize range as shown by HRTEM. They did not contain organic residues or any other iron (hydrous) oxide phase.

KW - HRTEM

KW - Magnetite

KW - Magnetometry

KW - Mössbauer

KW - XRD

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DO - 10.1016/j.matlet.2013.03.013

M3 - Article

AN - SCOPUS:84875735941

SN - 0167-577X

VL - 100

SP - 93

EP - 97

JO - Materials Letters

JF - Materials Letters

ER -

A novel route in the synthesis of magnetite nanoparticles

Abstract

Keywords

ASJC Scopus subject areas

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