A Peltier cooling diamond anvil cell for low-temperature Raman spectroscopic measurements

Naoki Noguchi; Takuo Okuchi

doi:10.1063/1.4972254

A Peltier cooling diamond anvil cell for low-temperature Raman spectroscopic measurements

Naoki Noguchi, Takuo Okuchi

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

A new cooling system using Peltier modules is presented for a low-temperature diamond anvil cell instrument. This cooling system has many advantages: it is vibration-free, low-cost, and compact. It consists of double-stacked Peltier modules and heat sinks, where a cooled ethylene glycol-water mixture flows through a chiller. Current is applied to the Peltier modules by two programmable DC power supplies. Sample temperature can be controlled within the range 210-300 K with a precision of ±0.1 K via a Proportional-Integral-Differential (PID) control loop. A Raman spectroscopic study for the H₂O ice VII-VIII transition is shown as an example of an application of the Peltier cooling diamond anvil cell system.

Original language	English
Article number	125107
Journal	Review of Scientific Instruments
Volume	87
Issue number	12
DOIs	https://doi.org/10.1063/1.4972254
Publication status	Published - Dec 1 2016

ASJC Scopus subject areas

Instrumentation

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10.1063/1.4972254

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abstract = "A new cooling system using Peltier modules is presented for a low-temperature diamond anvil cell instrument. This cooling system has many advantages: it is vibration-free, low-cost, and compact. It consists of double-stacked Peltier modules and heat sinks, where a cooled ethylene glycol-water mixture flows through a chiller. Current is applied to the Peltier modules by two programmable DC power supplies. Sample temperature can be controlled within the range 210-300 K with a precision of ±0.1 K via a Proportional-Integral-Differential (PID) control loop. A Raman spectroscopic study for the H2O ice VII-VIII transition is shown as an example of an application of the Peltier cooling diamond anvil cell system.",

author = "Naoki Noguchi and Takuo Okuchi",

note = "Funding Information: This work was financially supported by the Grants-in-Aid for Young Scientists (No. 15K17795) and Scientific Research (No. 26287135) from the Japan Society for the Promotion of Science. The authors thank two anonymous reviewers for helpful comments. Publisher Copyright: {\textcopyright} 2016 Author(s).",

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N2 - A new cooling system using Peltier modules is presented for a low-temperature diamond anvil cell instrument. This cooling system has many advantages: it is vibration-free, low-cost, and compact. It consists of double-stacked Peltier modules and heat sinks, where a cooled ethylene glycol-water mixture flows through a chiller. Current is applied to the Peltier modules by two programmable DC power supplies. Sample temperature can be controlled within the range 210-300 K with a precision of ±0.1 K via a Proportional-Integral-Differential (PID) control loop. A Raman spectroscopic study for the H2O ice VII-VIII transition is shown as an example of an application of the Peltier cooling diamond anvil cell system.

AB - A new cooling system using Peltier modules is presented for a low-temperature diamond anvil cell instrument. This cooling system has many advantages: it is vibration-free, low-cost, and compact. It consists of double-stacked Peltier modules and heat sinks, where a cooled ethylene glycol-water mixture flows through a chiller. Current is applied to the Peltier modules by two programmable DC power supplies. Sample temperature can be controlled within the range 210-300 K with a precision of ±0.1 K via a Proportional-Integral-Differential (PID) control loop. A Raman spectroscopic study for the H2O ice VII-VIII transition is shown as an example of an application of the Peltier cooling diamond anvil cell system.

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A Peltier cooling diamond anvil cell for low-temperature Raman spectroscopic measurements

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