TY - JOUR
T1 - Does 8-methacryloxyoctyl trimethoxy silane (8-MOTS) improve initial bond strength on lithium disilicate glass ceramic?
AU - Maruo, Yukinori
AU - Nishigawa, Goro
AU - Yoshihara, Kumiko
AU - Minagi, Shogo
AU - Matsumoto, Takuya
AU - Irie, Masao
N1 - Funding Information:
This work was partially supported by a Grant-in-aid for Scientific Research (KAKENHI), Grant Number 15K11159, from the Japan Society for the Promotion of Science (JSPS).
Publisher Copyright:
© 2016 The Academy of Dental Materials
PY - 2017/3/1
Y1 - 2017/3/1
N2 - Objectives Dental ceramic surfaces are modified with silane coupling agents, such as γ-methacryloxypropyl trimethoxy silane (γ-MPTS), to improve bond strength. For bonding between lithium disilicate glass ceramic and resin cement, the objective was to investigate if 8-methacryloxyoctyl trimethoxy silane (8-MOTS) could yield a similar performance as the widely used γ-MPTS. Methods One hundred and ten lithium disilicate glass ceramic specimens were randomly divided into 11 groups (n = 10) according to pretreatment regime. All specimens were pretreated with a different solution composed of one or a combination of these agents: 10 or 20 wt% silane coupling agent of γ-MPTS or 8-MOTS, followed by a hydrolysis solution of acetic acid or 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). Each pretreated surface was luted to a stainless steel rod of 3.6 mm diameter and 2.0 mm height with resin cement. Shear bond strength between ceramic and cement was measured after 24-h storage in 37 °C distilled water. Results 8-MOTS produced the same bonding performance as γ-MPTS. Both silane coupling agents significantly increased the bond strength of resin cement, depending on their concentration. When activated by 10-MDP hydrolysis solution, 20 wt% concentration produced the highest values (γ-MPTS: 24.9 ± 5.1 MPa; 8-MOTS: 24.6 ± 7.4 MPa). Hydrolysis with acetic acid produced lower bond strengths than with 10-MDP. Significance Silane coupling pretreatment with 8-MOTS increased the initial bond strength between lithium disilicate glass ceramic and resin cement, rendering the same bonding effect as the conventional γ-MPTS.
AB - Objectives Dental ceramic surfaces are modified with silane coupling agents, such as γ-methacryloxypropyl trimethoxy silane (γ-MPTS), to improve bond strength. For bonding between lithium disilicate glass ceramic and resin cement, the objective was to investigate if 8-methacryloxyoctyl trimethoxy silane (8-MOTS) could yield a similar performance as the widely used γ-MPTS. Methods One hundred and ten lithium disilicate glass ceramic specimens were randomly divided into 11 groups (n = 10) according to pretreatment regime. All specimens were pretreated with a different solution composed of one or a combination of these agents: 10 or 20 wt% silane coupling agent of γ-MPTS or 8-MOTS, followed by a hydrolysis solution of acetic acid or 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). Each pretreated surface was luted to a stainless steel rod of 3.6 mm diameter and 2.0 mm height with resin cement. Shear bond strength between ceramic and cement was measured after 24-h storage in 37 °C distilled water. Results 8-MOTS produced the same bonding performance as γ-MPTS. Both silane coupling agents significantly increased the bond strength of resin cement, depending on their concentration. When activated by 10-MDP hydrolysis solution, 20 wt% concentration produced the highest values (γ-MPTS: 24.9 ± 5.1 MPa; 8-MOTS: 24.6 ± 7.4 MPa). Hydrolysis with acetic acid produced lower bond strengths than with 10-MDP. Significance Silane coupling pretreatment with 8-MOTS increased the initial bond strength between lithium disilicate glass ceramic and resin cement, rendering the same bonding effect as the conventional γ-MPTS.
KW - Bond strength
KW - Lithium disilicate glass ceramic
KW - Silane coupling agent
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U2 - 10.1016/j.dental.2016.11.004
DO - 10.1016/j.dental.2016.11.004
M3 - Article
C2 - 27890356
AN - SCOPUS:85007170283
SN - 0109-5641
VL - 33
SP - e95-e100
JO - Dental Materials
JF - Dental Materials
IS - 3
ER -