Synthesis and crystal structure of 3-(4-Methoxyphenyl)-2- thioxo-2,3-dihydroquinazolin-4(1H)-one

Aamer Saeed; Shams ul Mahmood; H. Ishida

doi:10.3390/cryst1030171

Synthesis and crystal structure of 3-(4-Methoxyphenyl)-2- thioxo-2,3-dihydroquinazolin-4(1H)-one

Aamer Saeed, Shams ul Mahmood, H. Ishida

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P2₁ with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) Å, β = 97.752(3)°, V = 659.97(10) Å³, Z = 2.

Original language	English
Pages (from-to)	171-177
Number of pages	7
Journal	Crystals
Volume	1
Issue number	3
DOIs	https://doi.org/10.3390/cryst1030171
Publication status	Published - Aug 29 2011

Keywords

3-aryl-2-thioxo-2,3-dihydroquinazolin-4(1H)-ones
Quinazolinone
Synthesis

ASJC Scopus subject areas

Chemical Engineering(all)
Materials Science(all)
Condensed Matter Physics
Inorganic Chemistry

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10.3390/cryst1030171

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title = "Synthesis and crystal structure of 3-(4-Methoxyphenyl)-2- thioxo-2,3-dihydroquinazolin-4(1H)-one",

abstract = "Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21 with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) {\AA}, β = 97.752(3)°, V = 659.97(10) {\AA}3, Z = 2.",

keywords = "3-aryl-2-thioxo-2,3-dihydroquinazolin-4(1H)-ones, Quinazolinone, Synthesis",

author = "Aamer Saeed and {ul Mahmood}, Shams and H. Ishida",

year = "2011",

month = aug,

day = "29",

doi = "10.3390/cryst1030171",

language = "English",

volume = "1",

pages = "171--177",

journal = "Crystals",

issn = "2073-4352",

publisher = "Multidisciplinary Digital Publishing Institute (MDPI)",

number = "3",

}

TY - JOUR

T1 - Synthesis and crystal structure of 3-(4-Methoxyphenyl)-2- thioxo-2,3-dihydroquinazolin-4(1H)-one

AU - Saeed, Aamer

AU - ul Mahmood, Shams

AU - Ishida, H.

PY - 2011/8/29

Y1 - 2011/8/29

N2 - Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21 with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) Å, β = 97.752(3)°, V = 659.97(10) Å3, Z = 2.

AB - Synthesis of the title compound from 4-methoxyaniline was accomplished in three steps. The structure was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction data. It crystallizes in the monoclinic space group P21 with unit cell dimensions a = 9.9349(8), b = 6.3377(5), c = 10.5783(10) Å, β = 97.752(3)°, V = 659.97(10) Å3, Z = 2.

KW - 3-aryl-2-thioxo-2,3-dihydroquinazolin-4(1H)-ones

KW - Quinazolinone

KW - Synthesis

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DO - 10.3390/cryst1030171

M3 - Article

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VL - 1

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JO - Crystals

JF - Crystals

IS - 3

ER -

Synthesis and crystal structure of 3-(4-Methoxyphenyl)-2- thioxo-2,3-dihydroquinazolin-4(1H)-one

Abstract

Keywords

ASJC Scopus subject areas

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