Electrooxidation of alcohols in N-oxyl-immobilized silica gel/water disperse system: Approach to totally closed system

Manabu Kuroboshi; Kentaro Goto; Hideo Tanaka

doi:10.1055/s-0028-1087987

Electrooxidation of alcohols in N-oxyl-immobilized silica gel/water disperse system: Approach to totally closed system

Manabu Kuroboshi, Kentaro Goto, Hideo Tanaka

研究成果 › 査読

18 被引用数 (Scopus)

抄録

Electrooxidation of alcohols in a disperse system with N-oxyl-immobilized silica gel as a disperse phase and an aqueous NaBr/NaHCO₃ solution as a disperse medium proceeded smoothly to give the corresponding carbonyl compounds. The N-oxyl-immobilized silica gel 1 was prepared by silane-coupling method. Recycling of both the aqueous solution and the N-oxyl-immobilized silica gel 1 was performed successfully.

本文言語	English
論文番号	F20808SS
ページ（範囲）	903-908
ページ数	6
ジャーナル	Synthesis
号	6
DOI	https://doi.org/10.1055/s-0028-1087987
出版ステータス	Published - 3月 2009

ASJC Scopus subject areas

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有機化学

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10.1055/s-0028-1087987

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abstract = "Electrooxidation of alcohols in a disperse system with N-oxyl-immobilized silica gel as a disperse phase and an aqueous NaBr/NaHCO3 solution as a disperse medium proceeded smoothly to give the corresponding carbonyl compounds. The N-oxyl-immobilized silica gel 1 was prepared by silane-coupling method. Recycling of both the aqueous solution and the N-oxyl-immobilized silica gel 1 was performed successfully.",

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T2 - Approach to totally closed system

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AU - Goto, Kentaro

AU - Tanaka, Hideo

PY - 2009/3

Y1 - 2009/3

N2 - Electrooxidation of alcohols in a disperse system with N-oxyl-immobilized silica gel as a disperse phase and an aqueous NaBr/NaHCO3 solution as a disperse medium proceeded smoothly to give the corresponding carbonyl compounds. The N-oxyl-immobilized silica gel 1 was prepared by silane-coupling method. Recycling of both the aqueous solution and the N-oxyl-immobilized silica gel 1 was performed successfully.

AB - Electrooxidation of alcohols in a disperse system with N-oxyl-immobilized silica gel as a disperse phase and an aqueous NaBr/NaHCO3 solution as a disperse medium proceeded smoothly to give the corresponding carbonyl compounds. The N-oxyl-immobilized silica gel 1 was prepared by silane-coupling method. Recycling of both the aqueous solution and the N-oxyl-immobilized silica gel 1 was performed successfully.

KW - Alcohols

KW - Electron transfer

KW - Oxidations

KW - Solid-phase synthesis

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Electrooxidation of alcohols in N-oxyl-immobilized silica gel/water disperse system: Approach to totally closed system

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