One dimensional hydrogen bonded arrangement in new Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1): Synthesis, characterization, crystal structure and conformational studies

Aliakbar Dehno Khalaji; Hossein Mighani; Hamid Reza Bijanzadeh; Kazuma Gotoh; Hiroyuki Ishida

doi:10.1007/s10870-011-0133-4

One dimensional hydrogen bonded arrangement in new Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1): Synthesis, characterization, crystal structure and conformational studies

Aliakbar Dehno Khalaji, Hossein Mighani, Hamid Reza Bijanzadeh, Kazuma Gotoh, Hiroyuki Ishida

理学部

研究成果 › 査読

7 被引用数 (Scopus)

抄録

New Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1) was synthesized and characterized by elemental analyses, FT-IR and ¹H-NMR spectroscopy and single crystal X-ray diffraction. Molecular orbital calculation has been carried out for 1 by using HF method at 6-31G basis set. The title compound 1 crystallizes in monoclinic system, space group C2/c, with a = 19.4581(13) Å, b = 9.5805(5) Å, β = 93.471(2)°, V = 2575.9(3) Å³ and Z = 8. In the crystal structure two molecules are stabilized by a pair of intermolecular O1- H1•••N1ⁱ hydrogen bonds. The dimeric units are further linked via C6-H6•••O3ⁱⁱ hydrogen bond.

本文言語	English
ページ（範囲）	1515-1519
ページ数	5
ジャーナル	Journal of Chemical Crystallography
巻	41
号	10
DOI	https://doi.org/10.1007/s10870-011-0133-4
出版ステータス	Published - 10月 2011

ASJC Scopus subject areas

化学 (全般)
凝縮系物理学

文献へのアクセス

10.1007/s10870-011-0133-4

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引用スタイル

Khalaji, A. D., Mighani, H., Bijanzadeh, H. R., Gotoh, K., & Ishida, H. (2011). One dimensional hydrogen bonded arrangement in new Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1): Synthesis, characterization, crystal structure and conformational studies. Journal of Chemical Crystallography, 41(10), 1515-1519. https://doi.org/10.1007/s10870-011-0133-4

One dimensional hydrogen bonded arrangement in new Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1): Synthesis, characterization, crystal structure and conformational studies. / Khalaji, Aliakbar Dehno; Mighani, Hossein; Bijanzadeh, Hamid Reza その他.
In: Journal of Chemical Crystallography, Vol. 41, No. 10, 10.2011, p. 1515-1519.

研究成果 › 査読

Khalaji, AD, Mighani, H, Bijanzadeh, HR, Gotoh, K & Ishida, H 2011, 'One dimensional hydrogen bonded arrangement in new Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1): Synthesis, characterization, crystal structure and conformational studies', Journal of Chemical Crystallography, vol. 41, no. 10, pp. 1515-1519. https://doi.org/10.1007/s10870-011-0133-4

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abstract = "New Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1) was synthesized and characterized by elemental analyses, FT-IR and 1H-NMR spectroscopy and single crystal X-ray diffraction. Molecular orbital calculation has been carried out for 1 by using HF method at 6-31G basis set. The title compound 1 crystallizes in monoclinic system, space group C2/c, with a = 19.4581(13) {\AA}, b = 9.5805(5) {\AA}, β = 93.471(2)°, V = 2575.9(3) {\AA}3 and Z = 8. In the crystal structure two molecules are stabilized by a pair of intermolecular O1- H1•••N1i hydrogen bonds. The dimeric units are further linked via C6-H6•••O3ii hydrogen bond.",

keywords = "HF(6-31G), Hydrogen bonds, One-dimensional, Schiff-base, Spectroscopy",

author = "Khalaji, {Aliakbar Dehno} and Hossein Mighani and Bijanzadeh, {Hamid Reza} and Kazuma Gotoh and Hiroyuki Ishida",

note = "Funding Information: Acknowledgments We acknowledge Golestan University (GU) for partial support of this work, Tarbiat Modarres University (TMU) for NMR spectral analysis, and Okayama University (OU) for X-ray analysis.",

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AU - Ishida, Hiroyuki

N1 - Funding Information: Acknowledgments We acknowledge Golestan University (GU) for partial support of this work, Tarbiat Modarres University (TMU) for NMR spectral analysis, and Okayama University (OU) for X-ray analysis.

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AB - New Schiff-base compound (E)-2-(2,5-dimethoxybenzylideneamino)phenol (1) was synthesized and characterized by elemental analyses, FT-IR and 1H-NMR spectroscopy and single crystal X-ray diffraction. Molecular orbital calculation has been carried out for 1 by using HF method at 6-31G basis set. The title compound 1 crystallizes in monoclinic system, space group C2/c, with a = 19.4581(13) Å, b = 9.5805(5) Å, β = 93.471(2)°, V = 2575.9(3) Å3 and Z = 8. In the crystal structure two molecules are stabilized by a pair of intermolecular O1- H1•••N1i hydrogen bonds. The dimeric units are further linked via C6-H6•••O3ii hydrogen bond.

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